Glow Discharge Instructions =========================== .. note:: Note: Taken from https://www.dropbox.com/sh/rtss2c5qblmurmf/AABqRvU3X9eIrM7wiR3a9Jg1a?dl=0&preview=GLOW+DISCHARGE+INSTRUCTIONS.pdf Review and Update PELCO easiGlow™ --------------- * Switch on the machine and just click on `AUTO RUN`. The parameters that will be used are indicated in the screen. If you wish to change them just press `PROJ` and then change the parameters using the touch screen. * Useful parameters to change are the current and the time for glow discharge. The vacuum level to be reached is set to 0.39mBar. * You can decide also to run one of the preset programs. * To run a program press `MAIN` then select `PROTOCOLS` in the touch screen, then `RUN SCREEN` and `AUTORUN`. * There are 4 glow discharge programs with the following parameters: * PROGRAM 1. Glow discharge for 40 sec with a current of 20mA * PROGRAM 2. Glow discharge for 40 sec with a current of 15mA * PROGRAM 3. Glow discharge for 60 sec with a current of 20mA * PROGRAM 4. Glow discharge for 60 sec with a current of 21mA * When making graphene oxide you can use PROGRAM 4. * When glow discharging positively using amylamine a shorter time (PROGRAM 1 or 2) is recommended. Remember to run an empty run after you used amylamine. * Please do not change program setting without telling me. We can always decide to change these programs, but then we need to upgrade this sheet Quorum GloQube® Plus -------------------- * Switch on the machine using the main power switch at the back of the machine * **For air glow discharge** * **For glow discharge using a chimcal environment**